000 02164cam  2200349za 4500
0019.841556
003CaOODSP
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008170811s1972    onc     ob   f000 0 eng d
040 |aCaOODSP|beng
041 |aeng|bfre
043 |an-cn---
0861 |aM34-20/153E-PDF|zM34-20/153
1001 |aHitchen, A.
24514|aThe determination of titanium in lead zirconate-lead titanate electronic ceramics |h[electronic resource] : |ba comparison of titrimetric methods with polarographic and differential spectrophotometric methods / |cA. Hitchen, Extraction Metallurgy Division.
260 |aOttawa : |bInformation Canada, |c1972.
300 |aiv, 35 p.
4901 |aTechnical bulletin ; |vTB 153
500 |aCover title.
500 |a"October 1972."
500 |aDigitized edition from print [produced by Natural Resources Canada].
504 |aIncludes bibliographical references.
5203 |a“Three procedures for the determination of titanium in lead zirconate-lead titanate powders and process solutions which are simple, rapid, precise and accurate, are described. Two of the methods are based on reduction of the titanium with a) liquid zinc or lead amalgams or b) metallic aluminum, followed by titration of the reduced titanium with a standard ferric sulphate solution using sodium thiocyanate as the indicator. The third method is a polarographic procedure using an acetate + EDTA electrolyte. Relatively few elements interfere and procedures are suggested to overcome some of those that do. The accuracy and precision of the methods compare favourably with the much longer differential spectrophotometric method"--Abstract, p. i.
546 |aIncludes abstract in French.
69207|2gccst|aCeramics
69207|2gccst|aMetals
69207|2gccst|aAnalysis
7101 |aCanada. |bNatural Resources Canada.
7101 |aCanada. |bMines Branch.
830#0|aTechnical bulletin (Canada. Dept. of Energy, Mines and Resources. Mines Branch)|vTB 153|w(CaOODSP)9.834857
85640|qPDF|s1.16 MB|uhttps://publications.gc.ca/collections/collection_2017/rncan-nrcan/M34-20/M34-20-153-eng.pdf