000 02291cam  2200337za 4500
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008170725s1966    oncd    ob   f000 0 eng d
040 |aCaOODSP|beng
043 |an-cn---
0861 |aM38-8/24E-PDF|zM38-8/24
1001 |aKelly, F. J.
24514|aThe production of high-purity niobium oxide from pyrochlore-perovskite concentrate |h[electronic resource] / |cF.J. Kelly and W.A. Gow, Extraction Metallurgy Division.
260 |aOttawa : |bQueen's Printer, |c1966.
300 |a6 p. : |bcharts
4901 |aReprint series ; |vRS 24
500 |aCover title.
500 |a"Reprinted from the Canadian Mining and Metallurgical Bulletin, August, 1965."
500 |aHistorical publication digitized from print 2017 [by Natural Resources Canada].
504 |aIncludes bibliographical references.
5203 |a"A chemical process, based on laboratory investigations, is proposed for the production of high-purity niobium oxide from a pyrochlore-perovskite flotation concentrate produced from ore obtained at the Oka, Quebec, property of Columbium Mining Products Limited. The method developed included the decomposition and dissolution of the flotation concentrate with hot, concentrated sulphuric acid. The dissolved niobium was purified and concentrated by a solvent extraction step, using methyl isobutyl ketone as the extractant. The niobium was recovered from the extractant with ammonium fluoride solution from which niobium oxide was precipitated with ammonia. Finally, the filtered and washed precipitate was calcined. Ninety-six per cent of the niobium was recovered in a product analysing 99.9 per cent Nb2O5. The reagent cost was in the range of $1.00 to $1.25 per pound of niobium recovered"--Abstract, p. 1.
69207|2gccst|aMinerals
69207|2gccst|aProcessing
7001 |aGow, W. A.
7101 |aCanada. |bNatural Resources Canada.
7101 |aCanada. |bDepartment of Energy, Mines and Resources.
7101 |aCanada. |bMines Branch.
830#0|aReprint series - Dept. of Energy, Mines and Resources, Mines Branch ;|vRS 24|w(CaOODSP)9.834843
85640|qPDF|s2.40 MB|uhttps://publications.gc.ca/collections/collection_2017/rncan-nrcan/M38-8/M38-8-24-eng.pdf