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| 02936cam 2200421zi 4500 |
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| 001 | 9.873140 |
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| 003 | CaOODSP |
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| 005 | 20221107163830 |
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| 006 | m o d f |
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| 007 | cr ||||||||||| |
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| 008 | 190516e198812##oncad #ob f000 0 eng d |
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| 040 | |aCaOODSP|beng|erda|cCaOODSP |
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| 041 | |aeng|bfre |
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| 043 | |an-cn--- |
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| 086 | 1 |aEn13-5/88-110E-PDF |
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| 100 | 1 |aLee, H. B., |eauthor. |
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| 245 | 10|aChemical derivatization analysis of phenols. |nVI. |pDetermination of chlorinated phenolics in pulp and paper effluents / |cby Hing-Biu Lee, R.L. Hong-You, P.J.A. Fowlie. |
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| 246 | 10|aDetermination of chlorinated phenolics in pulp and paper effluents |
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| 264 | 1|aBurlington, Ontario, Canada : |bEnvironment Canada, National Water Research Institute, Research and Applications Branch, |cDecember 1988. |
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| 300 | |a1 online resource (20 pages, 5 unnumbered pages) : |billustrations, graphs. |
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| 336 | |atext|btxt|2rdacontent |
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| 337 | |acomputer|bc|2rdamedia |
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| 338 | |aonline resource|bcr|2rdacarrier |
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| 490 | 1 |aNWRI contribution ; |v88-110 |
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| 500 | |aDigitized edition from print [produced by Environment and Climate Change Canada]. |
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| 504 | |aIncludes bibliographical references. |
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| 520 | 3 |a"Based on the in-situ acetylation procedure, a method for the determination of 31 chlorinated phenolics in pulp and paper effluent samples has been successfully developed. Except for 4-chlorocatechol, this procedure provided satisfactory recovery for all phenols at three levels of fortification, namely, 400, 40, and 4 ug/L. Analysis of the acetyl derivatives was performed by gas chromatography using a 30 m DB-5 capillary column interfaced to an electron-capture detector. Mass spectral abundance data for the characteristic ions of the acetyl derivatives was acquired and used for the confirmation of compound identities. By operating a mass selective detector in the selected ion monitoring mode, application of this procedure was further extended to the mono chlorinated phenolics. Using a 50 mL effluent sample, the method detection limit was 0.5 ug/L for all except the monochlorinated compounds, which had a detection limit of 1 ug/L. Several effluent samples from a Canadian paper mill were analyzed by this procedure and the results are presented"--Abstract. |
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| 546 | |aIncludes abstract and management perspective in English and French. |
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| 692 | 07|2gccst|aPulp and paper industry |
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| 692 | 07|2gccst|aWaste management |
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| 692 | 07|2gccst|aAnalysis |
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| 700 | 1 |aHong-You, Robert L., |eauthor. |
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| 700 | 1 |aFowlie, Peter J. A., |eauthor. |
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| 710 | 1 |aCanada. |bEnvironment Canada. |
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| 710 | 2 |aNational Water Research Institute (Canada). |bResearch and Applications Branch. |
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| 830 | #0|aNWRI contribution ;|v88-110.|w(CaOODSP)9.844121 |
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| 856 | 40|qPDF|s1.45 MB|uhttps://publications.gc.ca/collections/collection_2019/eccc/en13-5/En13-5-88-110-eng.pdf |
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