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008240909e198611##nscad   ob   f000 0 eng d
040 |aCaOODSP|beng|erda|cCaOODSP
0411 |aeng|beng|bfre
0861 |aD68-21/13-1986E-PDF
1001 |aHiltz, John A., |eauthor.
24510|aOptimization of the Finnigan mat 5100 capillary gas chromatograph-mass spectrometer for the analysis of polychlorinated biphenyls / |cJ.A. Hiltz - J.J. Power ; approved by B.F. Peters.
264 1|aDartmouth, N.S. : |bNational Defence, Research and Development Branch, Defence Research Establishment Atlantic, |cNovember 1986.
300 |a1 online resource (v, 44 pages) : |billustrations, graphs.
336 |atext|btxt|2rdacontent
337 |acomputer|bc|2rdamedia
338 |aonline resource|bcr|2rdacarrier
4901 |aTechnical memorandum ; |v86/222
500 |aDigitized edition from print [produced by Defence Research and Development Canada].
504 |aIncludes bibliographical references (page 41).
5203 |a"The basis of operation of a capillary gas chromatograph with a quadrupole mass spectrometer as a detector is reviewed. This is followed by the description of the optimization of a Finnigan MAT 5100 gas chromatograph-mass spectrometer-data system (GC/MS/DS) for the detection and identification of PCBs. In particular, the effects of increasing electron multiplier voltage and the use of multiple ion detection (MID) scan sequences on the sensitivity of the quadrupole mass spectrometer are investigated. Both increasing the electron multiplier voltage and the use of specialized MID scan sequences were found to result in an improved detector response"--Abstract, page ii.
546 |aIncludes abstracts in English and French.
650 0|aPolychlorinated biphenyls.
650 0|aGas chromatography.
650 0|aMass spectrometry.
650 6|aBiphényles polychlorés.
650 6|aChromatographie en phase gazeuse.
650 6|aSpectrométrie de masse.
7102 |aDefence Research Establishment Atlantic, |eissuing body.
830#0|aD.R.E.A. technical memorandum ;|v86/222.|w(CaOODSP)9.941838
85640|qPDF|s1.60 MB|uhttps://publications.gc.ca/collections/collection_2024/rddc-drdc/D68-21-13-1986-eng.pdf