The determination of titanium in lead zirconate-lead titanate electronic ceramics : a comparison of titrimetric methods with polarographic and differential spectrophotometric methods / A. Hitchen, Extraction... : M34-20/153E-PDF
“Three procedures for the determination of titanium in lead zirconate-lead titanate powders and process solutions which are simple, rapid, precise and accurate, are described. Two of the methods are based on reduction of the titanium with a) liquid zinc or lead amalgams or b) metallic aluminum, followed by titration of the reduced titanium with a standard ferric sulphate solution using sodium thiocyanate as the indicator. The third method is a polarographic procedure using an acetate + EDTA electrolyte. Relatively few elements interfere and procedures are suggested to overcome some of those that do. The accuracy and precision of the methods compare favourably with the much longer differential spectrophotometric method"--Abstract, p. i.
Lien permanent pour cette publication :
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| Ministère/Organisme | Canada. Natural Resources Canada. Canada. Mines Branch. |
|---|---|
| Titre | The determination of titanium in lead zirconate-lead titanate electronic ceramics : a comparison of titrimetric methods with polarographic and differential spectrophotometric methods / A. Hitchen, Extraction Metallurgy Division. |
| Titre de la série | Technical bulletin ; TB 153 |
| Type de publication | Série - Voir l'enregistrement principal |
| Langue | [Anglais] |
| Format | Électronique |
| Document électronique | |
| Note(s) | Cover title. "October 1972." Digitized edition from print [produced by Natural Resources Canada]. Includes bibliographical references. Includes abstract in French. |
| Information sur la publication | Ottawa : Information Canada, 1972. |
| Auteur / Contributeur | Hitchen, A. |
| Description | iv, 35 p. |
| Numéro de catalogue |
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| Numéro de catalogue du ministère | 300037 |
| Descripteurs | Ceramics Metals Analysis |
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