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| 02962cam 2200445zi 4500 |
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| 001 | 9.877354 |
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| 003 | CaOODSP |
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| 005 | 20221107164944 |
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| 006 | m o d f |
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| 007 | cr bn||||||||| |
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| 008 | 190801s1993 onca ob f000 0 eng d |
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| 040 | |aCaOODSP|beng|erda|cCaOODSP |
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| 041 | 0 |aeng|beng|bfre |
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| 086 | 1 |aEn13-5/93-70E-PDF |
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| 100 | 1 |aOnuska, Francis I., |d1935- |eauthor. |
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| 245 | 10|aDetermination of toxaphene in soil by electron capture negative ion mass spectrometry and capillary column gas chromatography / |cF.I. Onuska, K.A. Terry, A. Seech and M. Antonic. |
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| 264 | 1|aBurlington, Ontario : |bNational Water Research Institute = Institut national de recherche sur les eaux, |c[1993] |
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| 300 | |a1 online resource (4 unnumbered pages, 13 pages, 3 unnumbered pages) : |billustrations. |
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| 336 | |atext|btxt|2rdacontent |
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| 337 | |acomputer|bc|2rdamedia |
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| 338 | |aonline resource|bcr|2rdacarrier |
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| 490 | 1 |aNWRI contribution ; |vno. 93-70 |
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| 500 | |aPage 12 blank and unnumbered in original print edition and omitted in this copy. |
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| 500 | |aDigitized edition from print [produced by Environment and Climate Change Canada]. |
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| 504 | |aIncludes bibliographical references (page 9). |
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| 520 | 3 |a"Although toxaphene is now limited in use, interest in its analysis continues because of its persistence and widespread atmospheric transport in the environment and its presence in many dump-sites all over the world. Top soil samples collected from a dump site were analyzed for toxaphene residues. Analyses were performed by wall-coated open tubular column (WCOT) gas chromatography in tandem with electron capture negative ion mass spectrometry (HRGC-ECNI-MS). Since the concentration of toxaphene residues were at mg/kg levels, the application of a mass spectrometer as a substance-selective detector has been applied. Advantages of this mode of real-time acquisition in continuous repetitive scanning of mass spectra has significant advantages in comparison to the selected ion monitoring technique. An average RSD of 10% and recoveries of 90 to 109% were obtained. Levels down to 50 µg/kg are obtainable"--Abstract. |
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| 546 | |aIncludes summaries and abstracts in English and French. |
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| 692 | 07|2gccst|aSoil |
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| 692 | 07|2gccst|aInsecticides |
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| 692 | 07|2gccst|aChemistry |
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| 700 | 1 |aTerry, K. A., |eauthor. |
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| 700 | 1 |aSeech, Alan G. |q(Alan George), |d1959- |eauthor. |
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| 700 | 1 |aAntonic, M., |eauthor. |
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| 710 | 1 |aCanada. |bEnvironment Canada. |
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| 710 | 2 |aNational Water Research Institute (Canada). |bResearch and Applications Branch. |
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| 710 | 2 |aGRACE Dearborn Inc. |bEnvironmental/Engineering Group. |
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| 710 | 2 |aNational Water Research Institute (Canada) |
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| 830 | #0|aNWRI contribution ;|vno. 93-70.|w(CaOODSP)9.844121 |
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| 856 | 40|qPDF|s1.65 MB|uhttps://publications.gc.ca/collections/collection_2019/eccc/en13-5/En13-5-93-70-eng.pdf |
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