Optimization of the Finnigan mat 5100 capillary gas chromatograph-mass spectrometer for the analysis of polychlorinated biphenyls / J.A. Hiltz - J.J. Power ; approved by B.F. Peters. : D68-21/13-1986E-PDF

"The basis of operation of a capillary gas chromatograph with a quadrupole mass spectrometer as a detector is reviewed. This is followed by the description of the optimization of a Finnigan MAT 5100 gas chromatograph-mass spectrometer-data system (GC/MS/DS) for the detection and identification of PCBs. In particular, the effects of increasing electron multiplier voltage and the use of multiple ion detection (MID) scan sequences on the sensitivity of the quadrupole mass spectrometer are investigated. Both increasing the electron multiplier voltage and the use of specialized MID scan sequences were found to result in an improved detector response"--Abstract, page ii.

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Renseignements sur la publication
Ministère/Organisme Defence Research Establishment Atlantic, issuing body.
Titre Optimization of the Finnigan mat 5100 capillary gas chromatograph-mass spectrometer for the analysis of polychlorinated biphenyls / J.A. Hiltz - J.J. Power ; approved by B.F. Peters.
Titre de la série Technical memorandum ; 86/222
Type de publication Série - Voir l'enregistrement principal
Langue [Anglais]
Format Électronique
Document électronique
Note(s) Digitized edition from print [produced by Defence Research and Development Canada].
Includes bibliographical references (page 41).
Includes abstracts in English and French.
Information sur la publication Dartmouth, N.S. : National Defence, Research and Development Branch, Defence Research Establishment Atlantic, November 1986.
Auteur / Contributeur Hiltz, John A., author.
Description 1 online resource (v, 44 pages) : illustrations, graphs.
Numéro de catalogue
  • D68-21/13-1986E-PDF
Descripteurs Polychlorinated biphenyls.
Gas chromatography.
Mass spectrometry.
Biphényles polychlorés.
Chromatographie en phase gazeuse.
Spectrométrie de masse.
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