Chemical derivatization analysis of phenols. VI. Determination of chlorinated phenolics in pulp and paper effluents / by Hing-Biu Lee, R.L. Hong-You, P.J.A. Fowlie.: En13-5/88-110E-PDF
"Based on the in-situ acetylation procedure, a method for the determination of 31 chlorinated phenolics in pulp and paper effluent samples has been successfully developed. Except for 4-chlorocatechol, this procedure provided satisfactory recovery for all phenols at three levels of fortification, namely, 400, 40, and 4 ug/L. Analysis of the acetyl derivatives was performed by gas chromatography using a 30 m DB-5 capillary column interfaced to an electron-capture detector. Mass spectral abundance data for the characteristic ions of the acetyl derivatives was acquired and used for the confirmation of compound identities. By operating a mass selective detector in the selected ion monitoring mode, application of this procedure was further extended to the mono chlorinated phenolics. Using a 50 mL effluent sample, the method detection limit was 0.5 ug/L for all except the monochlorinated compounds, which had a detection limit of 1 ug/L. Several effluent samples from a Canadian paper mill were analyzed by this procedure and the results are presented"--Abstract.
Permanent link to this Catalogue record:
publications.gc.ca/pub?id=9.873140&sl=0
| Department/Agency | Canada. Environment Canada. National Water Research Institute (Canada). Research and Applications Branch. |
|---|---|
| Title | Chemical derivatization analysis of phenols. VI. Determination of chlorinated phenolics in pulp and paper effluents / by Hing-Biu Lee, R.L. Hong-You, P.J.A. Fowlie. |
| Variant title | Determination of chlorinated phenolics in pulp and paper effluents |
| Series title | NWRI contribution ; 88-110 |
| Publication type | Series - View Master Record |
| Language | [English] |
| Format | Electronic |
| Electronic document | |
| Note(s) | Digitized edition from print [produced by Environment and Climate Change Canada]. Includes bibliographical references. Includes abstract and management perspective in English and French. |
| Publishing information | Burlington, Ontario, Canada : Environment Canada, National Water Research Institute, Research and Applications Branch, December 1988. |
| Author / Contributor | Lee, H. B., author. Hong-You, Robert L., author. Fowlie, Peter J. A., author. |
| Description | 1 online resource (20 pages, 5 unnumbered pages) : illustrations, graphs. |
| Catalogue number |
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| Subject terms | Pulp and paper industry Waste management Analysis |