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Chemical derivatization analysis of phenols. VI. Determination of chlorinated phenolics in pulp and paper effluents / by Hing-Biu Lee, R.L. Hong-You, P.J.A. Fowlie.: En13-5/88-110E-PDF

"Based on the in-situ acetylation procedure, a method for the determination of 31 chlorinated phenolics in pulp and paper effluent samples has been successfully developed. Except for 4-chlorocatechol, this procedure provided satisfactory recovery for all phenols at three levels of fortification, namely, 400, 40, and 4 ug/L. Analysis of the acetyl derivatives was performed by gas chromatography using a 30 m DB-5 capillary column interfaced to an electron-capture detector. Mass spectral abundance data for the characteristic ions of the acetyl derivatives was acquired and used for the confirmation of compound identities. By operating a mass selective detector in the selected ion monitoring mode, application of this procedure was further extended to the mono chlorinated phenolics. Using a 50 mL effluent sample, the method detection limit was 0.5 ug/L for all except the monochlorinated compounds, which had a detection limit of 1 ug/L. Several effluent samples from a Canadian paper mill were analyzed by this procedure and the results are presented"--Abstract.

Permanent link to this Catalogue record:
publications.gc.ca/pub?id=9.873140&sl=0

Publication information
Department/Agency
  • Canada. Environment Canada.
  • National Water Research Institute (Canada). Research and Applications Branch.
TitleChemical derivatization analysis of phenols. VI. Determination of chlorinated phenolics in pulp and paper effluents / by Hing-Biu Lee, R.L. Hong-You, P.J.A. Fowlie.
Variant title
  • Determination of chlorinated phenolics in pulp and paper effluents
Series title
  • NWRI contribution ; 88-110
Publication typeMonograph - View Master Record
Language[English]
FormatDigital text
Electronic document
Note(s)
  • Digitized edition from print [produced by Environment and Climate Change Canada].
  • Includes bibliographical references.
  • Includes abstract and management perspective in English and French.
Publishing information
  • Burlington, Ontario, Canada : Environment Canada, National Water Research Institute, Research and Applications Branch, December 1988.
Author / Contributor
  • Lee, H. B., author.
  • Hong-You, Robert L., author.
  • Fowlie, Peter J. A., author.
Description1 online resource (20 pages, 5 unnumbered pages) : illustrations, graphs.
Catalogue number
  • En13-5/88-110E-PDF
Subject terms
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