A multi-residue method for the determination of chlorobenzenes, PCB organochlorinated insecticides, PAH and chlorophenols in suspended sediments / by Hung Tse [and three others]. : En13-5/89-82E-PDF

"A multi-residue procedure was developed for the simultaneous determination of neutral and acidic environmental contaminants including polychlorinated biphenyls, organochlorinated insecticides, chlorobenzenes, polynuclear aromatic hydrocarbons, and chlorophenols in suspended sediments, at ng/g levels. This method involved an ultrasonic extraction of the sample sequentially at pH 7 and 2, silica gel column cleanup and fractionation, and final analysis by gas chromatography using electron-capture and mass spectrometric detectors. Six surrogates and one internal standard were added to the sample or the sample extract at various stages to monitor the recoveries of the analytes. Performance indicators such as method precision, accuracy and detection limits are presented. The procedure has been applied to the analysis of sediment samples in the Niagara River Water Quality Monitoring Program"--Abstract.

Lien permanent pour cette publication :
publications.gc.ca/pub?id=9.873598&sl=1

Renseignements sur la publication
Ministère/Organisme Canada. Environment Canada.
National Water Research Institute (Canada)
Titre A multi-residue method for the determination of chlorobenzenes, PCB organochlorinated insecticides, PAH and chlorophenols in suspended sediments / by Hung Tse [and three others].
Titre de la série NWRI contribution ; no. 89-82
Type de publication Série - Voir l'enregistrement principal
Langue [Anglais]
Format Électronique
Document électronique
Note(s) Digitized edition from print [produced by Environment and Climate Change Canada].
"February 1989."
Includes bibliographical references.
Includes abstract in French.
Information sur la publication Burlington, Ontario : National Water Research Institute, 1989.
Auteur / Contributeur Tse, Hung, author.
Description 1 online resource (18, (5) pages) : figures.
Numéro de catalogue
  • En13-5/89-82E-PDF
Descripteurs Water pollution
Sediments
Insecticides
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